Thionyl Chloride → HCID 12873573, 화합물
반응식
S(Cl)([Cl:3])=O.O[CH2:6][N:7]1[C:11]([CH3:13])([CH3:12])[C:10](=[O:14])[NH:9][C:8]1=[O:15]>C(Cl)Cl>[Cl:3][CH2:6][N:7]1[C:11]([CH3:13])([CH3:12])[C:10](=[O:14])[NH:9][C:8]1=[O:15]참가 물질
4
반응 조건
- 온도
- 25 °C
실험 절차
0.69 ml Thionyl chloride was added to a solution of 500 mg 1-Hydroxymethyl-5,5-dimethyl-imidazolidine-2,4-dione in 5 ml DCM at 0° C. for 30 minutes, then left to stir at 25° C. for 16 hours. The mixture was evaporated to dryness and used crude in the synthesis of example 23.
후처리
- waitleft
- customThe mixture was evaporated to dryness
- customin the synthesis of example 23
출처 및 근거
- ORD 기록
- ord-1503ffc39fd84a84ba289239b9d4477a
- 출처 데이터셋
- uspto-grants-2015_12
- 특허 번호
- US09199937B2
반응 노트
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