Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 1-(4-(3-Ethoxy-4-nitrophenyl)piperazin-1-yl)ethanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-Acetylpiperazine | HCID 83795 | — |
| 반응물 | 2-Ethoxy-4-fluoronitrobenzene | HCID 12918153 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1-(4-(3-Ethoxy-4-nitrophenyl)piperazin-1-yl)ethanone | HCID 118105754 | — |
반응 단계
The compound obtained in Step 1 above (300 mg), N-acetylpiperazine (300 mg), and potassium carbonate (500 mg) were dissolved in dimethylformamide (3 mL) and reacted at 80° C. overnight. The dimethylformamide of the reaction mixture was removed under reduced pressure, and added with water to form a solid. The solid was filtered to obtain a target compound as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09199944B2 |
| 출처 데이터셋 | uspto-grants-2015_12 |
| ORD ID | ord-2c8e1a83285440b6b1edfc06111e3ca8 |
| 출처 메모 | uspto-grants-2015_12 |