2,2-Dimethyloxan-4-ol → HCID 178426072, 화합물

HRID 1504396노트

반응식

HRID 1504396 반응식
[I-:1].[Zn+2:2].[I-].[CH3:4][C:5]1([CH3:12])[CH2:10][CH:9](O)[CH2:8][CH2:7][O:6]1>C1COCC1>[I-:1].[CH3:4][C:5]1([CH3:12])[CH2:10][CH:9]([Zn+:2])[CH2:8][CH2:7][O:6]1

참가 물질

4

반응물 2

HCID 49146922,2-Dimethyloxan-4-olHCID 9883512zinc(II)iodide

생성물 1

HCID 178426072HCID 178426072, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The title compound was prepared in an analogous, manner to tetrahydro-2H-pyran-4-yl)zinc(II) iodide except that 2,2-dimethyltetrahydro-2H-pyran-4-ol (Combi Blocks) was used instead of tetrahydro-2H-pyran-4-ol in Step 1 to afford a 0.24M solution of (2,2-dimethyltetrahydro-2H-pyran-4-yl)zinc(II) iodide in THF.

출처 및 근거

ORD 기록
ord-dfb1f2cab3de4b96972761228deb4140
출처 데이터셋
uspto-grants-2015_12
특허 번호
US09212182B2

반응 노트

불러오는 중…