Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Butyldiethanolamine → 6-Butyl-1,3,6-dioxazocan-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Butyldiethanolamine | HCID 7620 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Triphosgene | HCID 94429 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 6-Butyl-1,3,6-dioxazocan-2-one | HCID 118380294 | 239.2% |
반응 단계
The procedure of Example 1 was followed using N-butyl diethanolamine (13.5 g, 83.9 mmol), triethylamine (24.0 mL, 167.8 mmol), dry THF (600 mL) and triphosgene (8.3 g, 28.8 mmol). The filtrate was concentrated yielding a yellow/brown oil product (12.9 g, 82%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09215876B2 |
| 출처 데이터셋 | uspto-grants-2015_12 |
| ORD ID | ord-24c0c767132642f883f7580d4bab7314 |
| 출처 메모 | uspto-grants-2015_12 |