Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-tert-Butylcyclohexanone → 1-[4-(Tert-butyl)-1-cyclohexen-1-YL]pyrrolidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-tert-Butylcyclohexanone | HCID 7392 | — |
| 반응물 | Pyrrolidine | HCID 31268 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-[4-(Tert-butyl)-1-cyclohexen-1-YL]pyrrolidine | HCID 107232 | — |
반응 단계
A 50 mL round-bottomed flask containing 4-tert-butylcyclohexanone (6.01 gm) in anhydrous toluene (20 mL) was fitted with a Dean-Stark trap containing 3A molecular sieves, reflux condenser and a heating mantle. Pyrrolidine (6.00 mL) was added, and the solution heated to reflux for 18 hr. The solvent was evaporated and the crude product was used directly for the next reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09216966B2 |
| 출처 데이터셋 | uspto-grants-2015_12 |
| ORD ID | ord-bcf3b8f806d74b62bb2d057e7b5ce976 |
| 출처 메모 | uspto-grants-2015_12 |