Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methyl-3-nitroanisole → 5-Methoxy-o-toluidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methyl-3-nitroanisole | HCID 87137 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 5-Methoxy-o-toluidine | HCID 99500 | 98% |
반응 단계
A suspension of 1-methyl-4-(methyloxy)-2-nitrobenzene (20.0 g, 119.8 mmol) and Pd/C (10%, 3 g) in methanol (100 mL) was stirred under H2 atmosphere at room temperature overnight. The mixture was filtered through a pad of celite and the filtrate was evaporated under vacuum to afford the title compound as a solid (16.1 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09216967B2 |
| 출처 데이터셋 | uspto-grants-2015_12 |
| ORD ID | ord-8e86203e25ed4fb299a6b6dbffeed19f |
| 출처 메모 | uspto-grants-2015_12 |