Ammonia → HCID 90405643, 화합물
반응식
[CH3:1][O:2][C:3]1[C:11]([CH3:12])=[CH:10][CH:9]=[C:8]2[C:4]=1[CH:5]=[C:6]([C:13]([O:15]C)=O)[NH:7]2.[NH3:17]>CO>[CH3:1][O:2][C:3]1[C:11]([CH3:12])=[CH:10][CH:9]=[C:8]2[C:4]=1[CH:5]=[C:6]([C:13]([NH2:17])=[O:15])[NH:7]2참가 물질
4
실험 절차
80 mg of methyl 4-methoxy-5-methyl-1H-indole-2-carboxylate (0.39 mmol) was heated at 80 degrees in a sealed tube with 1 mL of 7M ammonia in methanol. After one week reaction the solvent evaporated to produce 79 mg of 4-methoxy-5-methyl-1H-indole-2-carboxamide that was used without purification in the next step.
후처리
- customAfter one week reaction the solvent
- customevaporated
출처 및 근거
- ORD 기록
- ord-7981d7b370454baf9dc58b1830e07515
- 출처 데이터셋
- uspto-grants-2015_12
- 특허 번호
- US09216993B2
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