Acetyl chloride → HCID 178496611, 화합물

HRID 1506250노트

반응식

HRID 1506250 반응식
[CH3:1][O:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([NH:9]C(=O)OC(C)(C)C)[CH2:5][CH2:4]1.C([Cl:20])(=O)C>C(O)C>[ClH:20].[CH3:1][O:2][C@H:3]1[CH2:8][CH2:7][C@H:6]([NH2:9])[CH2:5][CH2:4]1

참가 물질

4

반응물 2

HCID 6367Acetyl chlorideHCID 178496620HCID 178496620, 화합물

생성물 1

HCID 178496611HCID 178496611, 화합물수율 95%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

tert-Butyl (trans-4-methoxycyclohexyl)carbamate in ethanol (5 mL) was stirred with acetyl chloride (1.5 mL) for one day under cooling with ice, and the solvent was concentrated under reduced pressure to give the title compound (475 mg, yield 95%).

후처리

  1. temperatureunder cooling with ice
  2. concentrationthe solvent was concentrated under reduced pressure

출처 및 근거

ORD 기록
ord-6fa177b3cd6d47d3a0a132e1b3831867
출처 데이터셋
uspto-grants-2015_12
특허 번호
US09216999B2

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