HCID 70982893, 화합물 → 4-(Pyrrolidin-1-yl)butan-1-amine

HRID 1506752노트

반응식

HRID 1506752 반응식
[N:1]1([CH2:6][CH2:7][CH2:8][CH2:9][NH:10]C(=O)OCC2C=CC=CC=2)[CH2:5][CH2:4][CH2:3][CH2:2]1>[Pd]>[N:1]1([CH2:6][CH2:7][CH2:8][CH2:9][NH2:10])[CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

3

반응물 1

HCID 70982893HCID 70982893, 화합물

생성물 1

HCID 27627624-(Pyrrolidin-1-yl)butan-1-amine수율 82.2%

시약·촉매·용매 1

HCID 23938Palladium촉매

실험 절차

To a solution of benzyl 4-(pyrrolidin-1-yl)butylcarbamate (196 mg, 0.71 mmol) was added catalytic amount of Pd/C (5%). The reaction was stirred under a hydrogen atmosphere overnight and filtered. The filtrate was concentrated to give 4-(pyrrolidin-1-yl)butan-1-amine (83 mg)

후처리

  1. filtrationfiltered
  2. concentrationThe filtrate was concentrated

출처 및 근거

ORD 기록
ord-4bdf11b76ca04cc290690068dd55cd3a
출처 데이터셋
uspto-grants-2015_12
특허 번호
US09221760B2

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