Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Salvinorin B
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | Salvinorin A | HCID 128563 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Salvinorin B | HCID 11440685 | 42.3% |
반응 단계
To a solution of Salvinorin A (500 mg, 1.15 mM) in methanol (10 ml) was added solid sodium carbonate (490 mg, 4.6 mM) and the mixture stirred at room temperature overnight. Water (20 ml) was added to mixture and the mixture stirred for 30 mins. The solution was filtered and the filter-cake washed with ice-cold water (20 ml) and ice-cold methanol (20 ml) and dried in a dessicator to give Salvinorin B (191 mg, 42%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09222949B2 |
| 출처 데이터셋 | uspto-grants-2015_12 |
| ORD ID | ord-fde16edeb1b248fdb5fe3b8ab8ff05a5 |
| 출처 메모 | uspto-grants-2015_12 |