Neopentyl glycol → tert-Butyl 2-(3-hydroxy-2,2-dimethylpropoxymethyl)-6-methylbenzoate

HRID 15094

반응식

HRID 15094 반응식
Br[CH2:2][C:3]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:4]=1[C:5]([O:7][C:8]([CH3:11])([CH3:10])[CH3:9])=[O:6].[CH3:17][C:18]([CH3:23])([CH2:21][OH:22])[CH2:19][OH:20].OCCCOCC1C=CC=C(C)C=1C(OC(C)(C)C)=O>>[OH:20][CH2:19][C:18]([CH3:23])([CH3:17])[CH2:21][O:22][CH2:2][C:3]1[CH:15]=[CH:14][CH:13]=[C:12]([CH3:16])[C:4]=1[C:5]([O:7][C:8]([CH3:11])([CH3:10])[CH3:9])=[O:6]

참가 물질

4

반응물 3

HCID 31344Neopentyl glycolHCID 59341259Tert-butyl 2-(3-hydroxypropoxymethyl)-6-methylbenzoateHCID 59341261tert-Butyl 2-(bromomethyl)-6-methylbenzoate

생성물 1

HCID 59341262tert-Butyl 2-(3-hydroxy-2,2-dimethylpropoxymethyl)-6-methylbenzoate

실험 절차

tert-Butyl 2-(3-hydroxy-2,2-dimethylpropoxymethyl)-6-methylbenzoate is prepared from tert-butyl 2-bromomethyl-6-methylbenzoate and 2,2-dimethylpropane-1,3-diol in analogy to the synthesis of tert-butyl 2-(3-hydroxypropoxymethyl)-6-methylbenzoate.

출처 및 근거

ORD 기록
ord-567678157c9e4668a470f15f1995b5e5
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07732471B2

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