Stannous chloride dihydrate → ortho-aminophenylbenzoxazole
반응식
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]1[O:11][C:12]2[CH:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1)([O-])=O.O.O.Cl[Sn]Cl>C(O)C>[NH2:1][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]1[O:11][C:12]2[CH:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1참가 물질
4
반응 조건
- 온도
- 70 °C
실험 절차
A mixture of 8 g (0.033 mol) of 2-(2′-nitrophenyl)benzoxazole and 37.58 g (0.167 mol) of SnCl2.2H2O in 200 ml of ethanol was heated at 70° C. until the reaction was completely finished.
출처 및 근거
- ORD 기록
- ord-fac511347940456497d34748e92f3746
- 출처 데이터셋
- uspto-grants-2012_07
- 특허 번호
- US08216800B2
반응 노트
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