5-Hexen-1-ol → N-{[(Hex-5-en-1-yl)oxy]carbonyl}-3-methyl-L-valine

HRID 1511553노트

반응식

HRID 1511553 반응식
[CH3:1][C:2]([CH3:17])([CH3:16])[C@@H:3]([C:13]([OH:15])=[O:14])[NH:4][C:5]([O:7][CH2:8][CH2:9][CH2:10][CH:11]=[CH2:12])=[O:6].[CH2:18](O)CCCC=C>>[CH3:1][C:2]([CH3:17])([CH3:16])[C@@H:3]([C:13]([OH:15])=[O:14])[NH:4][C:5]([O:7][CH2:8][CH2:9][CH2:10][CH2:11][CH:12]=[CH2:18])=[O:6]

참가 물질

3

반응물 2

HCID 699635-Hexen-1-olHCID 453799283-Methyl-N-{[(pent-4-en-1-yl)oxy]carbonyl}-L-valine

생성물 1

HCID 45378514N-{[(Hex-5-en-1-yl)oxy]carbonyl}-3-methyl-L-valine

실험 절차

3-Methyl-N-[(hex-5-enyloxy)carbonyl]-L-valine was prepared according to the procedure for 3-methyl-N-[(pent-4-enyloxy)carbonyl]-L-valine by using 5-hexenol instead of 4-pentenol. LRMS (ESI) m/z 258 [(M+H)+; calcd for C13H24NO4: 258].

출처 및 근거

ORD 기록
ord-1b3eb219f2144c78b3e476f2ffe37789
출처 데이터셋
uspto-grants-2012_07
특허 번호
US08216999B2

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