2,2-Dimethylhex-5-en-1-ol → (2S)-({[(2,2-Dimethylhex-5-en-1-yl)oxy]carbonyl}amino)(1-methylcyclohexyl)acetic acid

HRID 1511581

반응식

HRID 1511581 반응식
CC(C)(C)[C@@H](C(O)=O)N[C:5](OCCCC=C)=[O:6].Cl.[NH2:19][C@@H:20]([C:24]1([CH3:30])[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]1)[C:21]([OH:23])=[O:22].[CH3:31][C:32]([CH3:39])([CH2:35][CH2:36][CH:37]=[CH2:38])[CH2:33][OH:34]>>[CH3:31][C:32]([CH3:39])([CH2:35][CH2:36][CH:37]=[CH2:38])[CH2:33][O:34][C:5]([NH:19][C@@H:20]([C:24]1([CH3:30])[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]1)[C:21]([OH:23])=[O:22])=[O:6]

참가 물질

4

반응물 3

HCID 102408212,2-Dimethylhex-5-en-1-olHCID 453799283-Methyl-N-{[(pent-4-en-1-yl)oxy]carbonyl}-L-valineHCID 57462912(S)-2-Amino-2-(1-methylcyclohexyl)acetic acid hydrochloride

생성물 1

HCID 45379613(2S)-({[(2,2-Dimethylhex-5-en-1-yl)oxy]carbonyl}amino)(1-methylcyclohexyl)acetic acid

실험 절차

(2S)-({[(2,2-Dimethylhex-5-en-1-yl)oxy]carbonyl}amino)(1-methylcyclohexyl)acetic acid was prepared according to the procedure for 3-methyl-N-[(pent-4-enyloxy)carbonyl]-L-valine using (2S)-amino(1-methylcyclohexyl)acetic acid-HCl and 2,2-dimethylhex-5-en-1-ol. LRMS (ESI) m/z 326.3 [(M+H)+; calcd for C18H32NO4: 326.2].

출처 및 근거

ORD 기록
ord-5683f704c6584a37a2ce6346ec4ca42e
출처 데이터셋
uspto-grants-2012_07
특허 번호
US08216999B2

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