Aluminium lithium hydride → (3-Fluoropyridin-4-yl)methanol

반응식

[F:1][C:2]1[CH:12]=[N:11][CH:10]=[CH:9][C:3]=1[C:4](OCC)=[O:5].[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[F:1][C:2]1[CH:12]=[N:11][CH:10]=[CH:9][C:3]=1[CH2:4][OH:5]

참가 물질

반응물 2

HCID 21226445Aluminium lithium hydride

HCID 46311382Ethyl 3-fluoroisonicotinate

생성물 1

HCID 49760376(3-Fluoropyridin-4-yl)methanol

실험 절차

The product of Example 129A and LiAlH4 were processed according to the method of Example 124B to provide the product. MS (ESI+) m/z 128 (M+H)+;

후처리

customto provide the product

출처 및 근거

ORD 기록: ord-229aca969a3848a7acb57c5d006fdd19
출처 데이터셋: uspto-grants-2012_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08217067B2

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