3-Bromo-3-methyl-1-butene → 1-[5-(4-Bromo-phenyl)-3-methyl-isoxazol-4-yl]-2,2-dimethyl-but-3-en-1-ol

반응식

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[CH:14]=[O:15])=[CH:4][CH:3]=1.Br[C:17]([CH3:21])([CH3:20])[CH:18]=[CH2:19]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[O:12][N:11]=[C:10]([CH3:13])[C:9]=2[CH:14]([OH:15])[C:17]([CH3:21])([CH3:20])[CH:18]=[CH2:19])=[CH:6][CH:7]=1

참가 물질

반응물 2

HCID 109536793-Bromo-3-methyl-1-butene

HCID 821337925-(4-Bromo-phenyl)-3-methyl-isoxazole-4-carbaldehyde

생성물 1

HCID 665821141-[5-(4-Bromo-phenyl)-3-methyl-isoxazol-4-yl]-2,2-dimethyl-but-3-en-1-ol

실험 절차

Prepared according to the procedure described in Example 63, Step 1, using 5-(4-bromo-phenyl)-3-methyl-isoxazole-4-carbaldehyde and 3-bromo-3-methyl-but-1-ene.

후처리

customPrepared

출처 및 근거

ORD 기록: ord-7617c7aa3626460a96369d9101b195b5
출처 데이터셋: uspto-grants-2012_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08217066B2

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