Chloroacetyl chloride → 4-chloro-N'-(2-chloroacetyl)benzohydrazide
반응식
[Cl:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([NH:8][NH2:9])=[O:7])=[CH:4][CH:3]=1.[Cl:12][CH2:13][C:14](Cl)=[O:15]>O1CCOCC1>[Cl:12][CH2:13][C:14]([NH:9][NH:8][C:6](=[O:7])[C:5]1[CH:10]=[CH:11][C:2]([Cl:1])=[CH:3][CH:4]=1)=[O:15]참가 물질
4
실험 절차
To a solution of p-chlorobenzoic hydrazide (11.2 g) in dioxane (100 ml) was added chloroacetyl chloride (6 ml). The resulting mixture was refluxed for three hours cooled to room temperature and filtered. The resulting solid was washed with ethyl ether and dried to yield N'-chloroacetyl-4-chlorobenzoic hydrazide as white solid.
후처리
- temperatureThe resulting mixture was refluxed for three hours
- filtrationfiltered
- washThe resulting solid was washed with ethyl ether
- customdried
출처 및 근거
- ORD 기록
- ord-5b77163772334a28b4e039cda3410b19
- 출처 데이터셋
- uspto-grants-1998_03
- 특허 번호
- US05726162
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