3,4-Dimethylaniline → 2-(2,6-Dimethylphenyl)-1H-indole-6-carboxylic acid (3,4-dimethylphenyl)-amide

참여 물질

반응 단계

The title compound was prepared from 2-(2,6-dimethylphenyl)-1H-indole-6-carboxylic acid and 3,4-dimethylaniline analogous to Example 3-4. 1H NMR (CDCl3, 400 MHz): δ 8.38 (s, broad, 1H), 8.08 (s, 1H), 7.84 (s, broad, 1H), 7.69 (d, J=8.3 Hz, 1H), 7.56 (dd, J=8.3, 1.6 Hz, 1H), 7.45 (d, J=2.0 Hz, 1H), 7.37 (dd, J=8.1, 2.3 Hz, 1H), 7.25 (m, 1H), 7.12 (m, 3H), 6.46 (m, 1H), 2.27 (s, 3H), 2.24 (s, 3H), 2.17 (s, 61-1). MS (m/z) 369.2 (M+1), Retention time=1.73 min (Method 10).

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