Methanol → Nitrophenoxyacetone

HRID 1515070

반응식

HRID 1515070 반응식
[N+:1]([C:4]1C=CC=[CH:11][C:5]=1[O:6]CC(=O)C)([O-:3])=[O:2].[C:15]1(C)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.C[OH:23]>>[N+:1]([CH:4]([O:23][C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1)[C:5](=[O:6])[CH3:11])([O-:3])=[O:2]

참가 물질

4

반응물 3

HCID 887MethanolHCID 1140TolueneHCID 792392-Propanone, 1-(2-nitrophenoxy)-

생성물 1

HCID 86645093Nitrophenoxyacetone

실험 절차

2624 g of o-nitrophenoxyacetone crystals (˜98%) from the 1st stage, step d), were dissolved at room temperature in a mixture of 11 307 g of methanol and 1290 g of toluene at 40° C., in order to obtain an about 17.6% solution of nitrophenoxyacetone.

출처 및 근거

ORD 기록
ord-4897176cdc784cb6a0b5a49820a27440
출처 데이터셋
uspto-grants-2012_07
특허 번호
US08222408B2

연결된 노트

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