Didecyldimethylammonium → HCID 178443399, 화합물

HRID 1517220노트

반응식

HRID 1517220 반응식
[CH2:1]([N+:11]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])([CH3:13])[CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[Na+]>O>[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[CH2:14]([N+:11]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])([CH3:13])[CH3:12])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]

참가 물질

4

반응물 2

HCID 16958DidecyldimethylammoniumHCID 16760658Sodium Salicylate

생성물 1

HCID 178443399HCID 178443399, 화합물수율 90%

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
60 °C

실험 절차

The stechiometric amounts of didecyldimethylammonium saccharinate and sodium salicylate were mixed in distilled water and stirred at 60° C. for 2 h. After that time the solution was cooled to room temperature. The product was extracted from the aqueous solution with chloroform. The chloroform phase was removed and solvent was evaporated. Synthesized didecyldimethylammonium salicylate (90% yield) was dried under vacuum.

후처리

  1. temperatureAfter that time the solution was cooled to room temperature
  2. extractionThe product was extracted from the aqueous solution with chloroform
  3. customThe chloroform phase was removed
  4. customsolvent was evaporated

출처 및 근거

ORD 기록
ord-0108f92853de4c5787c34919ef57250c
출처 데이터셋
uspto-grants-2012_07
특허 번호
US08232265B2

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