1-Chloro-3,5-dinitrobenzene → 1-Chloro-3-methoxy-5-nitrobenzene

HRID 1517950

반응식

HRID 1517950 반응식
[Cl:1][C:2]1[CH:7]=[C:6]([N+]([O-])=O)[CH:5]=[C:4]([N+:11]([O-:13])=[O:12])[CH:3]=1.[CH3:14][O-:15].[Na+]>CO>[Cl:1][C:2]1[CH:7]=[C:6]([O:15][CH3:14])[CH:5]=[C:4]([N+:11]([O-:13])=[O:12])[CH:3]=1

참가 물질

4

반응물 2

HCID 330981-Chloro-3,5-dinitrobenzeneHCID 10942334Sodium Methoxide

생성물 1

HCID 140260501-Chloro-3-methoxy-5-nitrobenzene

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

11.1 g 1-chloro-3,5-dinitrobenzene are dissolved in 100 ml of methanol and combined with 3 g sodium methoxide. Then the mixture is refluxed for 48 hours, cooled to ambient temperature and the solid is suction filtered.

후처리

  1. temperatureThen the mixture is refluxed for 48 hours
  2. filtrationfiltered

출처 및 근거

ORD 기록
ord-00a8e4c3ad574813b5d170d02c342a23
출처 데이터셋
uspto-grants-2012_07
특허 번호
US08232312B2

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