4-Methoxybenzenethiol → 1-Bromo-4-fluoro-2-(4-methoxy-phenylsulfanyl)-benzene

HRID 15203

반응식

HRID 15203 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([SH:9])=[CH:5][CH:4]=1.Br[C:11]1[CH:16]=[C:15]([F:17])[CH:14]=[CH:13][C:12]=1I.[Br:19]C1C=C(F)C=CC=1N>>[Br:19][C:12]1[CH:13]=[CH:14][C:15]([F:17])=[CH:16][C:11]=1[S:9][C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=1

참가 물질

4

반응물 3

HCID 127654-MethoxybenzenethiolHCID 2428732-Bromo-4-fluoroanilineHCID 27733722-Bromo-4-fluoro-1-iodobenzene

생성물 1

HCID 686816041-Bromo-4-fluoro-2-(4-methoxy-phenylsulfanyl)-benzene

실험 절차

Prepared from 4-methoxy-benzenethiol and 2-bromo-4-fluoro-1-iodo-benzene (prepared from 2-bromo-4-fluoro-phenylamine by diazotization according to the general procedure by Tunney and Stille J. Org. Chem. 1987, 52, 748-753)

출처 및 근거

ORD 기록
ord-83de2d79894e424182f94be9f49fe3bf
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07732463B2

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