Benzoylhydrazine → HCID 178487282, 화합물

HRID 1522985노트

반응식

HRID 1522985 반응식
[CH:1]1([CH2:7][CH2:8][N:9]2[C:19]3[C:14](=[CH:15][CH:16]=[C:17]([O:20][CH3:21])[CH:18]=3)[C:12](=O)[C:10]2=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:22]([NH:30][NH2:31])(=[O:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[CH:1]1([CH2:7][CH2:8][N:9]2[C:19]3[C:14](=[CH:15][CH:16]=[C:17]([O:20][CH3:21])[CH:18]=3)/[C:12](=[N:31]/[NH:30][C:22](=[O:29])[C:23]3[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=3)/[C:10]2=[O:11])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

3

반응물 2

HCID 11955BenzoylhydrazineHCID 25194458HCID 25194458, 화합물

생성물 1

HCID 178487282HCID 178487282, 화합물

실험 절차

The title compound was prepared as a yellow solid, using 1-(2-cyclohexylethyl)-6-methoxy-isatin and benzhydrazide according to the synthetic method E. NMR (CDCl3): δ 0.96-1.04 (m, 2H), 1.15-1.38 (m, 4H), 1.59 (dd, 2H), 1.65-1.75 (m, 3H), 1.81 (d, 2H), 3.74 (t, 2H), 3.87 (s, 3H), 6.43 (d, 1H), 6.64 (dd, 1H), 7.51 (t, 2H), 7.59 (t, 1H), 7.80 (d, 1H), 8.00 (d, 1H), 13.96 (br s, 1H).

출처 및 근거

ORD 기록
ord-d9fadffb8af34c2b912ffb305be9f7e7
출처 데이터셋
uspto-grants-2015_07
특허 번호
US09079854B2

반응 노트

불러오는 중…