Benzoylhydrazine → HCID 178495846, 화합물

HRID 1522996노트

반응식

[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6]([C:7](=O)[C:8](=[O:16])[N:9]2[CH2:12][CH2:13][O:14][CH3:15])=[CH:5][CH:4]=1.[C:18]([NH:26][NH2:27])(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH3:1][O:2][C:3]1[CH:11]=[C:10]2[C:6](/[C:7](=[N:27]/[NH:26][C:18](=[O:25])[C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)/[C:8](=[O:16])[N:9]2[CH2:12][CH2:13][O:14][CH3:15])=[CH:5][CH:4]=1

참가 물질

반응물 2

HCID 11955Benzoylhydrazine

HCID 25194459HCID 25194459, 화합물

생성물 1

HCID 178495846HCID 178495846, 화합물

실험 절차

The title compound was prepared as a yellow solid, using 6-methoxy-1-(2-methoxyethyl)-isatin and benzhydrazide according to the synthetic method NMR (CDCl3): δ 3.35 (s, 3H), 3.65 (t, 2H), 3.87 (s, 3H), 3.94 (t, 2H), 6.64 (d, 1H), 7.58 (t, 1H), 7.79 (d, 1H), 13.93 (br s, 1H).

출처 및 근거

ORD 기록: ord-3c4374304491452f8a1e3db73dd2a9ee
출처 데이터셋: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09079854B2

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