Ethanolamine → HCID 90312738, 화합물

HRID 1523768

반응식

HRID 1523768 반응식
[NH2:1][CH2:2][CH2:3][OH:4].[Br:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]([F:15])([F:14])[F:13])=[CH:8][C:7]=1[S:16](Cl)(=[O:18])=[O:17]>>[Br:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]([F:14])([F:13])[F:15])=[CH:8][C:7]=1[S:16]([NH:1][CH2:2][CH2:3][OH:4])(=[O:18])=[O:17]

참가 물질

3

반응물 2

HCID 700EthanolamineHCID 27786132-Bromo-5-(trifluoromethyl)benzene-1-sulfonyl chloride

생성물 1

HCID 90312738HCID 90312738, 화합물

실험 절차

The title compound was prepared in a manner similar to that described for Intermediate EU using 2-aminoethanol and 2-bromo-5-(trifluoromethyl)benzene-1-sulfonyl chloride. 1H NMR (500 MHz, CD3OD) δ 8.35-8.30 (m, 1H), 8.07-7.98 (dd, J=8.2, 0.9, 1H), 7.82-7.76 (m, 1H), 3.59-3.50 (t, J=5.9, 2H), 3.10-3.02 (t, J=5.9, 2H).

출처 및 근거

ORD 기록
ord-5240b594203846a78e746e45542479c6
출처 데이터셋
uspto-grants-2015_07
특허 번호
US09079866B2

연결된 노트

불러오는 중…