HCID 118232987, 화합물 → 3-(3-chloro-4-methyl-1H-pyrazol-1-yl)pyridine

HRID 1525774노트

반응식

HRID 1525774 반응식
[Cl:1][C:2]1[CH:6]([CH3:7])[CH2:5][N:4]([C:8]2[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=2)[N:3]=1>C(#N)C.[O-2].[Mn+4].[O-2]>[Cl:1][C:2]1[C:6]([CH3:7])=[CH:5][N:4]([C:8]2[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=2)[N:3]=1

참가 물질

4

반응물 1

HCID 118232987HCID 118232987, 화합물

생성물 1

HCID 216244353-(3-chloro-4-methyl-1H-pyrazol-1-yl)pyridine

시약·촉매·용매 2

HCID 178418406HCID 178418406, 화합물촉매HCID 6342Acetonitrile용매

반응 조건

온도
40 °C

실험 절차

In another embodiment, 3-(3-chloro-4-methyl-4,5-dihydro-1H-pyrazol-1-yl)pyridine (2) in acetonitrile is oxidized with manganese(IV) oxide and the mixture is heated at about 40° C. The 3-(3-chloro-4-methyl-1H-pyrazol-1-yl)pyridine (3) can be isolated and purified by standard techniques.

출처 및 근거

ORD 기록
ord-0d3d1ee38e4541febb05ef65477f742a
출처 데이터셋
uspto-grants-2015_07
특허 번호
US09085552B1

반응 노트

불러오는 중…