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Trifluoroacetic acid → (3-Aminomethyl-5-chloro-4-fluoro-phenyl)-diethyl-amine

HRID 1527479
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인쇄 미리보기

반응식

HRID 1527479 반응식
C(OC(=O)[NH:7][CH2:8][C:9]1[CH:14]=[C:13]([N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])[CH:12]=[C:11]([Cl:20])[C:10]=1[F:21])(C)(C)C.C(O)(C(F)(F)F)=O>C(Cl)Cl>[NH2:7][CH2:8][C:9]1[CH:14]=[C:13]([N:15]([CH2:18][CH3:19])[CH2:16][CH3:17])[CH:12]=[C:11]([Cl:20])[C:10]=1[F:21]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 6422Trifluoroacetic acidHCID 68283679(3-Chloro-5-diethylamino-2-fluoro-benzyl)-carbamic acid tert-butyl ester

생성물 1

HCID 71009409(3-Aminomethyl-5-chloro-4-fluoro-phenyl)-diethyl-amine

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

was prepared according to Scheme C1 (step B) from (3-chloro-5-diethylamino-2-fluoro-benzyl)-carbamic acid tert-butyl ester and TFA in CH2Cl2. MS (LC-MS): 231.0 [M]+; tR (HPLC conditions c): 2.29 min.

후처리

  1. customwas prepared
  2. custom2.29 min.

출처 및 근거

ORD 기록
ord-4aec3db98f8a4bc98b3ea59a082503b2
출처 데이터셋
uspto-grants-2015_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09085555B2

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