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HCID 178476752, 화합물 → Zinc Acetate

HRID 1527799
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HRID 1527799 반응식
[Zn:1](OC(C)=O)[O:2][C:3]([CH3:5])=[O:4].O.O>CO>[C:3]([O-:4])(=[O:2])[CH3:5].[Zn+2:1].[C:3]([O-:4])(=[O:2])[CH3:5]
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참가 물질

3

반응물 1

HCID 178476752HCID 178476752, 화합물

생성물 1

HCID 11192Zinc Acetate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

83.7 g of MeOH was added to Zn(OAc)2.2H2O (19.88 g) in a beaker to form 0.85 mol/L zinc acetate solution. 12.72 g of concentrated NaOH aqueous solution (49.8 wt %) was diluted with 83.7 g of MeOH followed by mixing with the Zn(OAc)2 solution under vigorous stirring. The reaction temperature of the system was maintained at 62° C. 4 minutes after the NaOH solution was mixed with the Zn(OAc)2 solution, 80 mL of 0.05 mol/L sodium oleate aqueous solution was added to the reaction solution. White precipitate formed almost immediately after the addition of sodium oleate. The reaction solution was aged at 62° C. for 45 minutes.

출처 및 근거

ORD 기록
ord-ee568a6d4aea49a2bf4e62db318f8359
출처 데이터셋
uspto-grants-2015_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09090468B2

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