1,2-Dibromoethane → HCID 67997599, 화합물

반응식

[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][S:9]([CH3:12])(=[O:11])=[O:10])=[N:6][CH:7]=1.Br[CH2:14][CH2:15]Br>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2([S:9]([CH3:12])(=[O:11])=[O:10])[CH2:15][CH2:14]2)=[N:6][CH:7]=1

참가 물질

반응물 2

HCID 78391,2-Dibromoethane

HCID 67997695HCID 67997695, 화합물

생성물 1

HCID 67997599HCID 67997599, 화합물수율 19%

실험 절차

The title compound was prepared from 5-bromo-2-methanesulfonylmethyl-pyridine and 1,2-dibromoethane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 19% of theory; LC (method 3): tR=2.52 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.

출처 및 근거

ORD 기록: ord-0cd3861758b54c989b8cf38acea4d91a
출처 데이터셋: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09090605B2

반응 노트

불러오는 중…