1,2-Dibromoethane → HCID 86696142, 화합물

반응식

[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][S:9]([CH3:12])(=[O:11])=[O:10])[N:3]=1.Br[CH2:14][CH2:15]Br>>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([C:8]2([S:9]([CH3:12])(=[O:11])=[O:10])[CH2:15][CH2:14]2)[N:3]=1

참가 물질

반응물 2

HCID 78391,2-Dibromoethane

HCID 59526086Pyridine, 2-bromo-6-[(methylsulfonyl)methyl]-

생성물 1

HCID 86696142HCID 86696142, 화합물수율 53%

실험 절차

The title compound was prepared from 2-bromo-6-methanesulfonylmethyl-pyridine and 1,2-dibromoethane following a procedure analogous to that described in Step 3 for Intermediate 4. Yield: 53% of theory; LC (method 3): tR=2.56 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.

출처 및 근거

ORD 기록: ord-3ffe6858742e4174bf06bd9512235032
출처 데이터셋: uspto-grants-2015_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09090605B2

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