Ethanol → Ethyl 1-(4-bromophenyl)cyclopropanecarboxylate
반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([C:11]([OH:13])=[O:12])[CH2:10][CH2:9]2)=[CH:4][CH:3]=1.S(=O)(=O)(O)O.[CH3:19][CH2:20]O>>[CH2:19]([O:12][C:11]([C:8]1([C:5]2[CH:4]=[CH:3][C:2]([Br:1])=[CH:7][CH:6]=2)[CH2:10][CH2:9]1)=[O:13])[CH3:20]참가 물질
4
반응 조건
- 온도
- 75 °C
실험 절차
1-(4-Bromo-phenyl)-cyclopropanecarboxylic acid (5 g, 20.7 mmol) in EtOH (50 mL) was treated with sulfuric acid (2 mL) and the reaction was stirred at 75° C. for 1 hour. Standard aqueous workup afforded title compound.
출처 및 근거
- ORD 기록
- ord-e22244131ba249b2b33f07765935f1dd
- 출처 데이터셋
- uspto-grants-2015_07
- 특허 번호
- US09090573B2
반응 노트
불러오는 중…