Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Dibromosalicylaldehyde → HCID 178449914, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Dibromosalicylaldehyde | HCID 7024 | — |
| 반응물 | N-tert-butylhydroxylamine | HCID 98586 | — |
| 생성물 | HCID 178449914 | HCID 178449914 | — |
반응 단계
The title compound was prepared according to the procedure described in Example 13 using 3,5-dibromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 111.3° C. (Rf=0.54 on a silica gel plate using 7:3 hexanes/EtOAc as an eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06197826B1 |
| 출처 데이터셋 | uspto-grants-2001_03 |
| ORD ID | ord-5175da832f654f48a85633dbe044f612 |
| 출처 메모 | uspto-grants-2001_03 |