Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Bromosalicylaldehyde → HCID 178449915, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Bromosalicylaldehyde | HCID 72863 | — |
| 반응물 | N-tert-butylhydroxylamine | HCID 98586 | — |
| 생성물 | HCID 178449915 | HCID 178449915 | — |
반응 단계
The title compound was prepared according to the procedure described in Example 1 using 5-bromo-2-hydroxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 68.7% yield as a yellow crystalline solid, m.p. 118.7° C. (Rf=0.65 on a silica gel plate using 1:1 EtOAc/hexanes as an eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06197826B1 |
| 출처 데이터셋 | uspto-grants-2001_03 |
| ORD ID | ord-de7a2748ebe648fd8b933d3c61c58394 |
| 출처 메모 | uspto-grants-2001_03 |