Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-bromobutanimide → Methyl 5-(bromomethyl)-2-methoxybenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | Methyl 2-methoxy-5-methylbenzoate | HCID 10241396 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | Methyl 5-(bromomethyl)-2-methoxybenzoate | HCID 19744340 | — |
반응 단계
A mixture of 2-methoxy-5-methylbenzoic acid methyl ester (J.Chem.Soc.Perkin Trans.1, 1994, 1125) (1.47 g) and N-bromosuccinimide (1.45 g) in benzene (15 ml) was irradiated under a 500 W halogen lamp for 3 hours. The solvent was evaporated and the residue triturated with diethyl ether. The succinimide was filtered off and the filtrate evaporated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06200981B1 |
| 출처 데이터셋 | uspto-grants-2001_03 |
| ORD ID | ord-cc5a220a1f5644198b9e4917cab8fd4f |
| 출처 메모 | uspto-grants-2001_03 |