Aniline → HCID 22993870, 화합물

HRID 1532003노트

반응식

HRID 1532003 반응식
[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([O:15][C:16]2[CH:21]=[C:20]([F:22])[CH:19]=[C:18]([F:23])[CH:17]=2)=[C:8]([CH:14]=1)[C:9]([O:11][CH2:12][CH3:13])=[O:10])([O-])=O.NC1C=CC=CC=1>C(O)C.C1COCC1>[NH2:1][C:4]1[CH:5]=[CH:6][C:7]([O:15][C:16]2[CH:17]=[C:18]([F:23])[CH:19]=[C:20]([F:22])[CH:21]=2)=[C:8]([CH:14]=1)[C:9]([O:11][CH2:12][CH3:13])=[O:10]

참가 물질

5

반응물 2

HCID 6115AnilineHCID 22993866HCID 22993866, 화합물

생성물 1

HCID 22993870HCID 22993870, 화합물수율 100.9%

시약·촉매·용매 2

HCID 702Ethanol용매HCID 8028Tetrahydrofuran용매

실험 절차

Using the method of Example 17.3, ethyl 5-nitro-2-(3,5-difluorophenoxy)benzoate (0.76 g) in ethanol (7 mL) and THF (3 mL) was converted to the corresponding aniline derivative which was obtained as an oil (0.696 g).

출처 및 근거

ORD 기록
ord-3923b9ac6b344a5a95188729cc6099ae
출처 데이터셋
uspto-grants-2001_03
특허 번호
US06200995B1

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