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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1532318생성일: 2026년 10월 26일

Calcium Hydroxide → 2-Chloro-5-methylsulphinyl-N-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamide

https://huagongshe.com/reaction/1532318

반응식

참여 물질

역할이름HCID투입량
반응물Calcium HydroxideHCID 6093208—
반응물2-Chloro-5-methylthio-N-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamideHCID 8923944—
반응물2-Chlorobenzene-1-carboperoxoic acidHCID 12587398—
용매ChloroformHCID 6212—
생성물2-Chloro-5-methylsulphinyl-N-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamideHCID 18381532110%

반응 단계

A solution of amide from Example 38 (0.2 g) in chloroform (5 ml) was treated with 70% m chloroperbenzoic acid (0.14 g). The reaction mixture was stirred for two days, calcium hydroxide (0.09 g) added and after stirring for a further 0.5 h the mixture was filtered. The filtrate was concentrated under reduced pressure to yield the sub-title product as a white solid (0.23 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06201024B1
출처 데이터셋uspto-grants-2001_03
ORD IDord-9e7c3ea9a8eb4df0897415036179a18f
출처 메모uspto-grants-2001_03