HCID 9801871, 화합물 → HCID 9824989, 화합물

HRID 1532643노트

반응식

HRID 1532643 반응식
[ClH:1].C(OCC)(=O)C.[CH3:8][N:9]([CH3:37])[CH2:10][CH2:11][CH2:12][N:13]1[C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=2[N:15]=[C:14]1[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>C(OCC)(=O)C>[ClH:1].[CH3:37][N:9]([CH3:8])[CH2:10][CH2:11][CH2:12][N:13]1[C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=2[N:15]=[C:14]1[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]

참가 물질

4

반응물 2

HCID 9801871HCID 9801871, 화합물HCID 21866389Hydrogen chloride-ethyl acetate

생성물 1

HCID 9824989HCID 9824989, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

4N Hydrochloric acid/ethyl acetate solution (0.13 ml) was added to a solution containing N,N-dimethyl-3-(2-pentadecyl-1H-benzimidazol-1-yl)-1-propanamine (0.20 g) in ethyl acetate (2 ml). After being stirred for 20 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with the mixed solution of ethyl acetate-hexane, thereby yielding the entitled compound (0.13 g) as white solid.

후처리

  1. concentrationthe reaction mixture was concentrated
  2. customThe residue was recrystallized with the mixed solution of ethyl acetate-hexane

출처 및 근거

ORD 기록
ord-20e82b5fab2649ee80729924cb92e72e
출처 데이터셋
uspto-grants-2001_03
특허 번호
US06204264B1

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