HCID 9846158, 화합물 → HCID 9869673, 화합물

HRID 1532645노트

반응식

HRID 1532645 반응식
[ClH:1].C(OCC)(=O)C.[CH2:8]([C:25]1[N:29]([CH2:30][CH2:31][CH2:32][N:33]([CH3:35])[CH3:34])[C:28]2[CH:36]=[CH:37][CH:38]=[CH:39][C:27]=2[N:26]=1)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>C(OCC)(=O)C>[ClH:1].[CH2:8]([C:25]1[N:29]([CH2:30][CH2:31][CH2:32][N:33]([CH3:34])[CH3:35])[C:28]2[CH:36]=[CH:37][CH:38]=[CH:39][C:27]=2[N:26]=1)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

참가 물질

4

반응물 2

HCID 9846158HCID 9846158, 화합물HCID 21866389Hydrogen chloride-ethyl acetate

생성물 1

HCID 9869673HCID 9869673, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

4N Hydrochloric acid/ethyl acetate solution (0.19 ml) was added to a solution containing 3-(2-heptadecyl-1H-benzimidazol-1-yl)-N,N-dimethyl-1-propanamine (0.33 g) in ethyl acetate (5 ml). After being stirred for 10 minutes at room temperature, the reaction mixture was concentrated. The residue was recrystallized with ethyl acetate, thereby yielding the entitled compound (0.32 g) as white solid.

후처리

  1. concentrationthe reaction mixture was concentrated
  2. customThe residue was recrystallized with ethyl acetate

출처 및 근거

ORD 기록
ord-9200d9f4de064ba08d6153b591ed8acc
출처 데이터셋
uspto-grants-2001_03
특허 번호
US06204264B1

반응 노트

불러오는 중…