HCID 3635836, 화합물 → HCID 22013772, 화합물

HRID 1532652노트

반응식

HRID 1532652 반응식
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=2[N+:17]([O-])=O)[CH2:3][CH2:2]1>C(O)C.[C].[Pd]>[O:1]1[CH2:2][CH2:3][N:4]([CH2:7][CH2:8][CH2:9][NH:10][C:11]2[C:12]([NH2:17])=[CH:13][CH:14]=[CH:15][CH:16]=2)[CH2:5][CH2:6]1

참가 물질

4

반응물 1

HCID 3635836HCID 3635836, 화합물

생성물 1

HCID 22013772HCID 22013772, 화합물수율 72.3%

시약·촉매·용매 2

HCID 178418390HCID 178418390, 화합물촉매HCID 702Ethanol용매

실험 절차

10% of palladium-carbon (0.237 g) was added to a solution containing N-(3-morpholinopropyl)-2-nitroaniline (1.040 g) in ethanol (12 ml) and the mixture was stirred for 7 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (0.667 g) as blackish brown solid.

후처리

  1. customAfter the catalyst was removed out by filtration
  2. concentrationthe filtrate was concentrated

출처 및 근거

ORD 기록
ord-1a6fd057d8774fbebee166422eacf186
출처 데이터셋
uspto-grants-2001_03
특허 번호
US06204264B1

반응 노트

불러오는 중…