HCID 22013755, 화합물 → HCID 22013764, 화합물
반응식
[CH3:1][N:2]([CH3:21])[CH2:3][CH2:4][CH2:5][NH:6][C:7]1[CH:17]=[CH:16][C:10]([C:11]([N:13]([CH3:15])[CH3:14])=[O:12])=[CH:9][C:8]=1[N+:18]([O-])=O>C(O)C.[C].[Pd]>[NH2:18][C:8]1[CH:9]=[C:10]([CH:16]=[CH:17][C:7]=1[NH:6][CH2:5][CH2:4][CH2:3][N:2]([CH3:1])[CH3:21])[C:11]([N:13]([CH3:15])[CH3:14])=[O:12]참가 물질
4
실험 절차
10% of palladium-carbon (0.56 g) was added to a solution containing 4-{[3-(dimethylamino)propyl]amino}-N,N-dimethyl-3-nitrobenzamide (2.82 g) in ethanol (20 ml) and the mixture was stirred for 13 hours under a hydrogen gas atmosphere at room temperature. After the catalyst was removed out by filtration, the filtrate was concentrated, thereby yielding the entitled compound (2.59 g) as dark red solid.
후처리
- customAfter the catalyst was removed out by filtration
- concentrationthe filtrate was concentrated
출처 및 근거
- ORD 기록
- ord-77bacec6fc0045a8a6f9f93863987be3
- 출처 데이터셋
- uspto-grants-2001_03
- 특허 번호
- US06204264B1
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