Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(4-Ethylaminophenyl)-4-phenylmethylpiperazine → 1-(4-Ethylaminophenyl)piperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(4-Ethylaminophenyl)-4-phenylmethylpiperazine | HCID 19911465 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-(4-Ethylaminophenyl)piperazine | HCID 19911458 | — |
반응 단계
A solution of 1-(4-ethylaminophenyl)-4-phenylmethylpiperazine in ethanol is catalytically hydrogenated at about 70° C. and 50 p.s.i., in the presence of 10% palladium on carbon. After hydrogen uptake ceases, the catalyst is removed by filtration and the filtrate concentrated to obtain the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05086055 |
| 출처 데이터셋 | uspto-grants-1992_02 |
| ORD ID | ord-590c27b31dff476298179a48dbf18bb1 |
| 출처 메모 | uspto-grants-1992_02 |