HCID 54392015, 화합물 → 1,2-Difluoro-3-propylbenzene
반응식
[H][H].[CH:3]([C:6]1[C:7]([F:13])=[C:8]([F:12])[CH:9]=[CH:10][CH:11]=1)=[CH:4][CH3:5]>C1COCC1.[Pd]>[CH2:3]([C:6]1[C:7]([F:13])=[C:8]([F:12])[CH:9]=[CH:10][CH:11]=1)[CH2:4][CH3:5]참가 물질
5
실험 절차
Hydrogen is introduced at room temperature until saturation into a solution of 0.13 mol of 3-propenyl-1,2-difluorobenzene (obtainable according to Example 11) in 100 ml of THF containing 5 g of suspended Pd/C. Customary working up is carried out after stirring for 3 hours, b.p.30 : 72° C.
후처리
- custom72° C.
출처 및 근거
- ORD 기록
- ord-c3f34e8f179a421b85029ea005840929
- 출처 데이터셋
- uspto-grants-1992_02
- 특허 번호
- US05087764
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