Methanesulfonic Acid → HCID 13131214, 화합물

HRID 1534633노트

반응식

HRID 1534633 반응식
O[CH2:2][C:3]([NH:6][C:7]([CH3:12])([CH2:10][CH3:11])[CH2:8][OH:9])([CH3:5])[CH3:4].CS(O)(=O)=O>>[CH3:12][C:7]1([CH2:10][CH3:11])[CH2:8][O:9][CH2:2][C:3]([CH3:5])([CH3:4])[NH:6]1

참가 물질

4

반응물 2

HCID 6395Methanesulfonic AcidHCID 131312092-[(1-Hydroxy-2-methylpropan-2-yl)amino]-2-methylbutan-1-ol

생성물 1

HCID 13131214HCID 13131214, 화합물수율 50%

시약·촉매·용매 1

HCID 178435178HCID 178435178, 화합물용매

실험 절차

In a manner analogous to that described in example 5A hereinabove, starting with (1-hydroxy-2-methyl-2-propyl)(1-hydroxy-2-methyl-2-butyl)amine and reacting with methanesulfonic acid, then working up the reaction mixture, a colorless oil having a bp 71°-3° C./20 mm, is obtained in about 50% yield. Less than 5% by weight of the oil is found to provide excellent u-v light stability in polypropylene.

후처리

  1. customis obtained in about 50% yield

출처 및 근거

ORD 기록
ord-7bc5bbe50ee343a3a32f6eb654d0bd53
출처 데이터셋
uspto-grants-1992_02
특허 번호
US05089614

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