Formaldehyde → n-Hexylhydroxymethylphosphinic acid, n-butyl ester

반응식

[CH2:1]([PH:7](=[O:13])[O:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[CH2:14]=[O:15]>>[CH2:1]([P:7]([CH2:14][OH:15])(=[O:13])[O:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

참가 물질

반응물 2

HCID 712Formaldehyde

HCID 178418254HCID 178418254, 화합물

생성물 1

HCID 86752200n-Hexylhydroxymethylphosphinic acid, n-butyl ester

실험 절차

The title compound was prepared from n-hexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

후처리

customPurification by chromatography
washeluting with dichloromethane containing 5% methanol
customgave an oil

출처 및 근거

ORD 기록: ord-8ac817860d9d44d4acd7988671266af2
출처 데이터셋: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05726165

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