Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Thioglycolate → Methyl 1,3-dioxa-5-thia-s-indacene-6-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Thioglycolate | HCID 16907 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 1,3-Benzodioxole-5-carboxaldehyde, 6-bromo- | HCID 95062 | — |
| 생성물 | Methyl 1,3-dioxa-5-thia-s-indacene-6-carboxylate | HCID 11746624 | — |
반응 단계
Using 3.0 g (13.1 mmol) of 6-bromopiperonal, 0.79 g (19.7 mmol) of sodium hydride (60% pure) and 1.53 g (14.4 mmol) of methyl mercaptoacetate, 732 mg (18.5% of theory) of the title compound are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07732477B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-1d37e20f6bc1493e953b8cdd50446e3e |
| 출처 메모 | uspto-grants-2010_06 |