Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Bicarbonate → (3,3-Diethoxy-propyl)-carbamic acid allyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | 1-Amino-3,3-diethoxypropane | HCID 521029 | — |
| 반응물 | But-3-enoyl Chloride | HCID 10975427 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | (3,3-Diethoxy-propyl)-carbamic acid allyl ester | HCID 86605042 | — |
반응 단계
But-3-enoyl chloride (930 uL, 8.84 mmol) was added slowly to a rapidly stirring mixture of 3,3-diethoxy-propylamine (1.0 g, 6.80 mmol) and NaHCO3 (2 mL of 0.6 M NaHCO3 in water) in DCM (100 mL). The reaction was stirred at room temperature overnight, then partitioned between water and DCM. The organic layer was washed several times with water and concentrated to give the crude sub-title compound that was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07732618B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-233d52f44e6349a7a7bc1dd57e6b77de |
| 출처 메모 | uspto-grants-2010_06 |