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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 15532생성일: 2026년 10월 25일

(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl ester → HCID 67199974, 화합물

https://huagongshe.com/reaction/15532

반응식

참여 물질

역할이름HCID투입량
반응물(4-tert-Butoxycarbonylamino-2-nitro-phenylamino)-acetic acid tert-butyl esterHCID 67201113—
촉매PalladiumHCID 23938—
용매EthanolHCID 702—
생성물HCID 67199974HCID 67199974—

반응 단계

The product of step b.) (2.0 g, 5.45 mmol) was stirred with 3% Pd/C (200 mg) in ethanol (20 mL) under H2 (1 atm) for 90 minutes. The reaction was filtered over celite and concentrated to dryness to give the sub-title compound as a brown oil. This compound was used in crude form without purification. MS: ESI (positive): 338 (M+H).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07732618B2
출처 데이터셋uspto-grants-2010_06
ORD IDord-87a849f7a0c44fe2bcd1487199a27e08
출처 메모uspto-grants-2010_06