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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 15583생성일: 2026년 10월 25일

Trifluoroacetic acid → HCID 59342528, 화합물

https://huagongshe.com/reaction/15583

반응식

참여 물질

역할이름HCID투입량
반응물Trifluoroacetic acidHCID 6422—
반응물{5-[Benzyl-(3-methyl-butyryl)-amino]-2-propyl-benzoimidazol-1-yl}-acetic acid tert-butyl esterHCID 67200170—
생성물HCID 59342528HCID 59342528—

반응 단계

{5-[Benzyl-(3-methyl-butyryl)-amino]-2-propyl-benzoimidazol-1-yl}-acetic acid tert-butyl ester (0.12 mmol) was treated with TFA (2 mL) for 2 hours, concentrated, and purified by preparative LCMS to give the title compound. 1H NMR (d6-DMSO) δ7.48 (d, 1H), 7.21 (m, 6H), 6.92 (m, 1H), 5.08 (s, 2H), 4.89 (s, 2H), 2.72 (t, 2H), 2.00 (m, 3H), 1.71 (m, 2H), 0.99 (t, 3H), 0.79 (m, 6H). MS calculated for C24H29N3O3+H: 408, observed: 408.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07732618B2
출처 데이터셋uspto-grants-2010_06
ORD IDord-e6da319626d14f84a34f18a106491a97
출처 메모uspto-grants-2010_06