참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | O-Xylene | HCID 7237 | — |
| 반응물 | 2-Nitroamino-2-imidazoline | HCID 410042 | — |
| 반응물 | 2-Amino-1-(4-methylphenyl)ethan-1-ol | HCID 3519929 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | alpha-(2-Imidazolin-2-ylaminomethyl)-p-methylbenzyl alcohol | HCID 53928717 | — |
반응 단계
A mixture of 9.06 parts of α-(aminomethyl)-p-methylbenzyl alcohol, 7.8 parts of 2-(nitramino)-2-imidazoline and 8 parts of xylene is stirred for 30 minutes at 160°C (oil-bath). The reaction mixture is cooled and acetone is added. The precipitated product is filtered off, washed with acetone and dried, yielding α-(2-imidazolin-2-ylaminomethyl)-p-methylbenzyl alcohol; 163.7°C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03983133 |
|---|
| 출처 데이터셋 | uspto-grants-1976_09 |
|---|
| ORD ID | ord-c621f94f9ce7425795b4c019eb926d30 |
|---|
| 출처 메모 | uspto-grants-1976_09 |
|---|
