Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(4-Methoxyphenyl)but-3-en-2-one → 6,10,10-Trimethyl-8-(4'-methoxyphenyl)pyrido[1,2-a]indolium perchlorate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(4-Methoxyphenyl)but-3-en-2-one | HCID 95414 | — |
| 반응물 | 3H-Indole, 2,3,3-trimethyl-, perchlorate | HCID 14913188 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 6,10,10-Trimethyl-8-(4'-methoxyphenyl)pyrido[1,2-a]indolium perchlorate | HCID 12374368 | — |
반응 단계
2,3,3-Trimethyl-3H-indolium perchlorate (5 g.) and 4-p-methoxyphenylbut-3-ene-2-one (10 g.) were heated together on the steam bath for three hours. The cooled mixture was diluted with methanol and filtered. The product was purified by recrystallization from acetonitrile. Yield 4.1 g.; m.p. 298°-300° .
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03983288 |
| 출처 데이터셋 | uspto-grants-1976_09 |
| ORD ID | ord-10a387c8143d4b76b6e143ffaefdfae1 |
| 출처 메모 | uspto-grants-1976_09 |